SamplePreparationTypically,titaniumandzirconiumsamplesarechemicallyetchedtoremovesurfacecontaminationwhenoxygenandnitrogenaredetermined.However,etchingcanintroducehydrogenintothesample.ASTMmethodE1409"DeterminationofOxygenandNitrogeninTitaniumandTitaniumAlloysbytheInertGasFusionTechnique",asupdatedin1996,permitseitheretchingorabrading(filing)ofthetestspecimen.ASTME1447"DeterminationofHydrogeninTitaniumandTitaniumAlloysbytheInertGasFusionThermalConductivity/InfraredDetectionMethod"permitssurfacepreparationbyabrading(ifnecessarytoremovecontamination).DifferencesinsamplepreparationpresentsomewhatofadilemmaregardingsimultaneousdeterminationofO,N,andHintitanium.However,abradingsampleswithafiletoremovesurfacecontaminationwillyieldaccurateO,N,andHresults.TheONH836utilizesahigh-powerelectrodefurnacetoquicklyandefficientlyreleasethetargetgasesfromwithinthesample,whichallowsforaveryrapidsimultaneousdeterminationofoxygen,nitrogen,andhydrogen.上海禹重实业有限公司为您提供分析仪,欢迎您的来电哦!北京美国LECO分析仪厂家供应
Procedure–Powder/ChipSamplesDeterminetheinstrumentblank.PresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.Cleantheupperandlowerelectrodeeithermanuallyorremovethecrucibleandpresstheanalyzebuttontocleanwithanautomaticcleanerifapplicable.Addapproximately0.05gof***GraphitePowdertoa782-720GraphiteCrucible.Firmlyplacethecrucibleonthelowerelectrodetiporappropriateautoloaderposition.进口分析仪厂家供应分析仪,就选上海禹重实业有限公司,让您满意,有想法可以来我司咨询!
Procedure–Powder/ChipSamplesInstrumentcalibration/driftcorrection.Addapproximately0.05gof***GraphitePowdertoa***GraphiteCrucible.Firmlyplacethecrucibleonthelowerelectrodetiporappropriateautoloaderposition.PresstheAnalyzebuttonontheinstrumentscreen,thelowerelectrodewillcloseandtheanalysissequencewillstartandendautomatically.Repeatsteps3bthrough3iaminimumofthreetimesforeachcalibration/driftstandardused.
氧氮氢分析仪的常见故障及解决方法:氧和氮空白值超过20。这是由于气流小,不能将炉子中的空气驱赶出去。可调节气体流量,调节载气压力在0.2~0.4MPa。接通仪器载气,放一个石墨坩埚在下电极上,打开主电源开关,点击软件上的关炉按钮,关闭炉子并等待10s。调节流量调节器,直到流量计a显示为30L/h,打开炉子。调节调节器直到流量计b显示为50L/h,再次关闭炉子。如果以上设置不稳定,则增加流量至100L/h,反复调节直至仪器稳定。上海禹重实业有限公司是一家专业提供分析仪的公司,有想法的可以来电咨询!
LECO—YoursourcefortotalanalyticalsolutionsCSCS844and744Series:Carbon/SulfurbyCombustionCarbonandsulfurdeterminationbycombustioninfrareddetectionQuick,accurate,andaffordabledeterminationforbothproductioncontrolandresearchCalibration,analysis,evaluation,anddiagnosticfunctionsaccessibleviauser-friendlybrandsoftwareGDSGDS500Aand850AAtomicEmissionSpectrometersSpectralrangefrom120to800nmContinuousprofileofconcentration/thicknessLarge,dynamicrangewithconcentrationsfromppmto100%byweightShortanalysistime(minutes)上海禹重实业有限公司是一家专业提供分析仪的公司,期待您的光临!江苏LECO分析仪供应商
分析仪,就选上海禹重实业有限公司。北京美国LECO分析仪厂家供应
User-FriendlyBrandSoftwareCornerstoneLECOsexclusivebrandsoftwareenablestheusertohavecompleteaccesstoanalysisCornerstonecontrol,methodsettings,diagnostics,reporting,andmoreinahighlyorganizedandimmersiveenvironment.Designedthroughacollaborationofcustomerfeedbackandinnovativeengineering,Cornerstoneallowstheusertoconductalloftheirday-to-dayoperationswithinasingleAnalysisscreendesignedforspeedandease-of-use.Ourinnovativegroupingofsampledataintosetsandreplicatessimplifiesthedataoutputandautomaticallycalculatesrelevantstatistics,alleviatingtheneedforadditionaldataprocessing.北京美国LECO分析仪厂家供应
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