Procedure - Solid Samples
Instrument calibration/drift correction.
Add approximately 0.05 g of *** Graphite Powder to a *** Graphite Crucible.
Firmly place the crucible on the lower electrode tip or appropriate autoloader position.
Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically.
Repeat steps 3b through 3j a minimum of three times for each calibration/drift standard used.
Calibrate/drift following the procedure outlined in the operator's instruction manual.
Instrument Highlights and Features
Features and Benefits
LED light ring illuminates the furnace area
Choice of either argon or helium carrier gas
Novel electrode design increases heat transfer efficiency for increased stability
Non-touch interface systems are also available
User-friendly brand software
High-Performance Detector Design
Thermostatic construction provides increased protection from ambient temperature fluctuations
Optimized emitter control and detection circuitryimproves the IR cell lifetime and long-term stability,
resulting in superior accuracy and precision
Infrared detection for the determination of oxygen, thermoconductivity detection for the determination
of nitrogen
山东进口分析仪厂家报价减少了繁琐的额外数据处理。
Procedure - Solid Samples
Press the Analyze button on the instrument screen again, the loading head slide-block will close and the lower electrode will open.
Clean the upper and lower electrode manually, or, if applicable, remove the crucible and press the analyze button to clean with the automatic cleaner
Add approximately 0.05 g of *** Graphite Powder to a *** Graphite Crucible.
Firmly place the crucible on the lower electrode tip or appropriate autoloader position.
Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically
美国力可LECO氧氮氢分析仪
公司介绍:
美国力可公司(LECO)始于1936年 ,以生产用于冶金、机械、能源、化工、农业、食品及科研开发领域的各种分析仪器。
ONH836氧气/氮气/氢气元素分析仪设计用于使用惰性气体熔融技术对无机材料,铁和非铁合金以及耐火材料中的氧,氮和氢含量进行宽范围的测量。
坚固的样品加载区域可简化日常维护并大程度减少大气污染
用于氧气检测的三重红外电池可实现业内大的检测范围
通过自动化选项提高实验室生产率
可用的自动清洁器大程度地减少了两次分析之间的手动清洁需求
适用于坩埚和样品的20位往复式装载机
安装在动臂上的触摸屏界面可提供更好的人体工程学设计和直观的操作
红外(IR)和热导率(TC)检测器,没有活动部件,也无需手动调节
改善TC电池的稳定性
可绕过的OMI-2载气洗涤塔,提高了TC电池的稳定性
获得Dyanamic流量补偿可进一步增强TC细胞的稳定性
氧氮氢分析仪怎么选?欢迎联系上海禹重科技,我司产品质量保证,欢迎咨询!
Sample Preparation
Sampling and sample preparation is an important issue because traditional methods used to obtain samples for oxygen and nitrogen determination are different from those recommended for hydrogen, especially when sampling molten metal. The main difference in steel sampling procedures for oxygen/nitrogen and hydrogen is due to the mobilityof hydrogen. Special precautions must be used when sampling for hydrogen. From molten steel and iron, a sample must be quickly quenched in cold water and chilled in a refrigerant such as liquefied nitrogen or a mixture of acetone and solid carbon dioxide in order to reduce losses of hydrogen from diffusion. Losses of oxygen and nitrogen from diffusion are not a problem. A sample that is taken for hydrogen and
chilled in a refrigerant can also be used for oxygen and nitrogen determination. However, a sample that is typically taken for oxygen and/or nitrogen determination is not suitable for hydrogen determination due to hydrogen loss (diffusion). Surface contamination must be removed by filing or light grinding, using care not to overheat the sample.
20位试样自动进样系统。浙江美国LECO分析仪采购
力可***仪器采用触摸屏技术和在线软件平台,增强了仪器的可操作性、降低了分析成本、节省实验室桌面空间。浙江分析仪厂家报价
Method Selection
Two methods are described in this application note; either method can be used to analyze iron, steel, nickel-, and cobalt-base alloys. The Precision Method is recommended for general use and will provide the best precision and accuracy throughout the typical O, N, and H concentrations found in this group of metals; approximate cycle time is 3.5 minutes. The Fast Track method can be used where speed of analysis is a critical component; for example, when molten metal is being sampled and results are required in the shortest possible time. This method will produce suitable results for most samples; approximate cycle time is 2.25 minutes. As noted above, sampling and sample preparation are key elements to accurate O, N, and Hdetermination as well. It is up to the user to determine which method best meets their needs.
浙江分析仪厂家报价
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